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AS ISO 10414.1:2022
$272.87
Petroleum and natural gas industries – Field testing of drilling fluids, Part 1: Water-based fluids
AS ISO 10414.1:2022 identically adopts ISO 10414 1:2008, which provides standard procedures for determining the characteristics of water-based drilling fluids, including: drilling fluid density (mud weight); viscosity and gel strength; filtration; water, oil and solids contents; sand content; methylene blue capacity; pH; alkalinity and lime content; chloride content; and total hardness as calcium.
Table of contents
Header
About this publication
Preface
Foreword
Introduction
1 Scope
2 Terms and definitions
3 Symbols and abbreviated terms
3.1 Symbols
3.2 Abbreviations
4 Drilling fluid density (mud weight)
4.1 Principle
4.2 Apparatus
4.2.1
4.2.2
4.3 Procedure
4.3.1
4.3.2
4.3.3
4.3.4
4.3.5
4.3.6
4.4 Calculation
4.4.1
4.4.2
5 Alternative drilling fluid density method
5.1 Principle
5.2 Apparatus
5.2.1
5.2.2
5.3 Procedure
5.3.1
5.3.2
5.3.3
5.3.4
5.3.5
5.3.6
5.3.7
5.3.8
5.3.9
5.4 Calculation
6 Viscosity and gel strength
6.1 Principle
6.2 Determination of viscosity using the Marsh funnel
6.2.1 Apparatus
6.2.1.1
6.2.1.1.1
6.2.1.1.2
6.2.1.1.3
6.2.1.2
6.2.1.3
6.2.1.4
6.2.2 Procedure
6.2.2.1
6.2.2.2
6.2.2.3
6.2.2.4
6.3 Determination of viscosity and/or gel strength using a direct-indicating viscometer
6.3.1 Apparatus
6.3.1.1
6.3.1.2
6.3.1.3
6.3.1.4
6.3.2 Procedure
6.3.2.1
6.3.2.2
6.3.2.3
6.3.2.4
6.3.2.5
6.3.2.6
6.3.2.7
6.3.3 Calculation
7 Filtration
7.1 Principle
7.2 Low-temperature/low-pressure test
7.2.1 Apparatus
7.2.1.1
7.2.1.2
7.2.1.3
7.2.2 Procedure
7.2.2.1
7.2.2.2
7.2.2.3
7.2.2.4
7.2.2.5
7.2.2.6
7.2.2.7
7.3 High-temperature/high-pressure (HTHP) test
7.3.1 Apparatus
7.3.1.1
7.3.1.2
7.3.1.2.1
7.3.1.2.2
7.3.1.3
7.3.1.4
7.3.1.5
7.3.1.6
7.3.2 Procedure for temperatures to 150 °C (300 °F)
7.3.2.1
7.3.2.2
7.3.2.3
7.3.2.4
7.3.2.5
7.3.2.6
7.3.2.7
7.3.2.8
7.3.2.9
7.3.2.10
7.3.2.11
7.3.2.12
7.3.3 Procedure for temperatures above 150 °C (300 °F)
7.3.3.1
7.3.3.2
7.3.3.3
7.3.3.4
7.3.3.5
7.3.3.6
7.3.3.7
7.3.3.8
7.3.3.9
7.3.3.10
7.3.3.11
7.3.3.12
7.3.3.13
8 Water, oil and solids contents
8.1 Principle
8.2 Apparatus
8.2.1
8.2.1.1
8.2.1.2
8.2.1.3
8.2.1.4
8.2.2
8.2.3
8.2.4
8.2.5
8.2.6
8.2.7
8.2.8
8.2.9
8.3 Procedure
8.3.1
8.3.2
8.3.3
8.3.4
8.3.5
8.3.6
8.3.7
8.3.8
8.3.9
8.3.10
8.3.11
8.3.12
8.3.13
8.3.14
8.4 Calculation
8.4.1
8.4.2
8.4.3
8.4.4
8.4.5
9 Sand content
9.1 Principle
9.2 Apparatus
9.2.1
9.2.2
9.2.3
9.3 Procedure
9.3.1
9.3.2
9.3.3
9.3.4
10 Methylene blue capacity
10.1 Principle
10.1.1
10.1.2
10.1.3
10.2 Reagents and apparatus
10.2.1
10.2.2
10.2.3
10.2.4
10.2.5
10.2.6
10.2.7
10.2.8
10.2.9
10.2.10
10.3 Procedure
10.3.1
10.3.2
10.3.3
10.3.4
10.4 Calculation
11 pH
11.1 Principle
11.1.1
11.1.2
11.1.3
11.2 Reagents and apparatus
11.2.1
11.2.2
11.2.3
11.2.4
11.2.5
11.2.6
11.2.7
11.2.8
11.2.9
11.2.10
11.2.11
11.2.12
11.3 Procedure for pH measurement
11.3.1
11.3.2
11.3.3
11.3.4
11.3.5
11.3.6
11.3.7
11.3.8
11.3.9
11.3.10
11.3.11
11.3.12
11.3.13
11.3.14
11.3.15
11.4 Care of electrode
11.4.1
11.4.2
11.4.3
11.4.4
11.4.5
11.4.6
12 Alkalinity and lime content
12.1 Principle
12.1.1
12.1.2
12.1.3
12.1.4
12.2 Reagents and apparatus
12.2.1
12.2.2
12.2.3
12.2.4
12.2.5
12.2.6
12.2.7
12.2.8
12.2.9
12.3 Procedure — Phenolphthalein and methyl orange filtrate alkalinities
12.3.1
12.3.2
12.3.3
12.3.4
12.4 Procedure — Phenolphthalein drilling fluid alkalinity
12.4.1
12.4.2
12.5 Calculation of ion concentrations from Pf and Mf
12.6 Estimation of lime content
12.6.1
12.6.2
13 Chloride ion content
13.1 Principle
13.2 Reagents and apparatus
13.2.1
13.2.2
13.2.3
13.2.4
13.2.5
13.2.6
13.2.7
13.2.8
13.2.9
13.3 Procedure
13.3.1
13.3.2
13.4 Calculation
13.4.1
13.4.2
13.4.3
14 Total hardness as calcium
14.1 Principle
14.2 Reagents and apparatus
14.2.1
14.2.2
14.2.3
14.2.4
14.2.5
14.2.6
14.2.7
14.2.8
14.2.9
14.2.10
14.2.11
14.2.12
14.3 Procedure
14.3.1
14.3.2
14.3.3
14.3.4
14.3.5
14.3.6
14.3.7
14.3.8
14.4 Calculation
Annex A
A.1 Calcium
A.1.1 Principle
A.1.2 Reagents and apparatus
A.1.2.1
A.1.2.2
A.1.2.3
A.1.2.4
A.1.2.5
A.1.2.6
A.1.2.7
A.1.2.8
A.1.2.9
A.1.2.10
A.1.2.11
A.1.2.12
A.1.2.13
A.1.3 Procedure
A.1.3.1
A.1.3.2
A.1.3.3
A.1.3.4
A.1.3.5
A.1.3.6
A.1.3.7
A.1.3.8
A.1.4 Calculation
A.2 Magnesium
A.2.1 Principle
A.2.2 Procedure
A.2.2.1
A.2.2.2
A.2.3 Calculation
A.3 Calcium sulfate
A.3.1 Principle
A.3.2 Reagents and apparatus
A.3.2.1
A.3.2.2
A.3.2.3
A.3.2.4
A.3.2.5
A.3.2.6
A.3.2.7
A.3.2.8
A.3.2.9
A.3.2.10
A.3.2.11
A.3.2.12
A.3.2.13
A.3.2.14
A.3.3 Procedure
A.3.3.1
A.3.3.2
A.3.3.3
A.3.4 Calculation
A.3.4.1
A.3.4.2
A.4 Sulfide
A.4.1 Principle
A.4.1.1
A.4.1.2
A.4.2 Reagents and apparatus
A.4.2.1
A.4.2.2
A.4.2.3
A.4.2.4
A.4.2.4.1
A.4.2.4.2
A.4.2.5
A.4.2.6
A.4.2.7
A.4.2.8
A.4.3 Procedure
A.4.3.1
A.4.3.2
A.4.3.3
A.4.3.4
A.4.3.5
A.4.3.6
A.4.3.7
A.4.3.8
A.4.3.9
A.4.3.10
A.4.3.11
A.4.3.12
A.4.3.13
A.4.3.14
A.4.3.15
A.4.3.16
A.4.3.17
A.4.4 Calculation
A.5 Carbonate
A.5.1 Principle
A.5.2 Reagents and apparatus
A.5.2.1
A.5.2.2
A.5.2.3
A.5.2.4
A.5.2.5
A.5.2.6
A.5.2.7
A.5.2.8
A.5.2.9
A.5.2.10
A.5.3 Procedure
A.5.3.1
A.5.3.2
A.5.3.3
A.5.3.4
A.5.3.5
A.5.3.6
A.5.3.7
A.5.3.8
A.5.3.9
A.5.3.10
A.5.3.11
A.5.3.12
A.5.3.13
A.5.3.14
A.5.3.15
A.5.3.16
A.5.3.17
A.5.4 Calculation
A.6 Potassium (concentration above 5 000 mg/l)
A.6.1 Principle
A.6.2 Reagents and apparatus
A.6.2.1
A.6.2.2
A.6.2.3
A.6.2.4
A.6.2.5
A.6.2.6
A.6.2.7
A.6.3 Preparation of standard calibration curve
A.6.3.1
A.6.3.2
A.6.3.3
A.6.3.4
A.6.3.5
A.6.3.6
A.6.3.7
A.6.4 Test procedure
A.6.4.1
A.6.4.2
A.6.4.3
A.6.4.4
A.6.4.5
A.6.4.6
A.6.5 Calculation
A.7 Potassium (concentration below 5 000 mg/l)
A.7.1 Principle
A.7.2 Reagents and apparatus
A.7.2.1
A.7.2.2
A.7.2.3
A.7.2.4
A.7.2.5
A.7.2.6
A.7.2.7
A.7.2.8
A.7.2.9
A.7.2.10
A.7.3 Procedure
A.7.3.1
A.7.3.2
A.7.3.3
A.7.3.4
A.7.3.5
A.7.3.6
A.7.3.7
A.7.4 Calculation
Annex B
B.1 Principle
B.1.1
B.1.2
B.2 Apparatus
B.2.1
B.2.2
B.2.3
B.2.4
B.3 Procedure
B.3.1
B.3.2
B.3.3
B.4 Calculation
B.4.1
B.4.2
Annex C
C.1 Principle
C.2 Apparatus
C.2.1
C.2.2
C.2.3
C.2.4
C.2.5
C.3 Procedure
C.3.1
C.3.2
C.3.3
C.3.4
C.3.5
C.4 Calculation
C.4.1
C.4.2
C.4.3
Annex D
D.1 Principle
D.2 Apparatus
D.2.1
D.2.2
D.3 Procedure
D.3.1
D.3.2
D.3.3
D.3.4
D.3.5
D.3.6
D.3.7
D.3.8
Annex E
E.1 Principle
E.1.1
E.1.2
E.2 Reagents and apparatus
E.2.1
E.2.2
E.2.3
E.2.4
E.2.5
E.2.6
E.2.7
E.2.8
E.2.9
E.2.10
E.3 Procedure
E.3.1
E.3.2
E.3.3
E.3.4
E.3.5
E.4 Comments on visual examination
E.4.1
E.4.2
E.4.3
E.5 Calculation
E.5.1
Annex F
F.1 General
F.2 Sampling of powdered material in packages
F.2.1
F.2.2
F.2.3
F.3 Sampling of powdered material in bulk
F.3.1
F.3.2
F.3.3
F.4 Preparation of test sample
F.4.1
F.4.2
F.5 Test
F.6 Inspection
F.7 Rejection
F.8 Retesting
F.8.1
F.8.2
Annex G
G.1 General
G.2 Bottom-flow sampling (preferred)
G.2.1 Apparatus
G.2.1.1
G.2.1.2
G.2.1.3
G.2.2 Procedure
G.2.2.1
G.2.2.2
G.2.2.3
G.2.2.4
G.2.2.5
G.3 Grab sampling
G.3.1 Apparatus
G.3.1.1
G.3.1.2
G.3.2 Procedure
G.3.2.1
G.3.2.2
G.3.2.3
G.3.2.4
Annex H
H.1 General
H.2 Calibration of apparatus
H.2.1 Volumetric glassware
H.2.2 Thermometers
H.2.3 Viscometer
H.2.4 Drilling fluid balance
H.2.5 Retort-kit cup
H.3 Procedure for calibration
H.3.1 Liquid receivers
H.3.1.1
H.3.1.2
H.3.1.3
H.3.1.4
H.3.1.5
H.3.2 Thermometers
H.3.2.1
H.3.2.2
H.3.2.3
H.3.2.4
H.3.2.5
H.3.2.6
H.3.2.7
H.3.3 Viscometers
H.3.3.1
H.3.3.2
H.3.3.3
H.3.3.4
H.3.3.5
H.3.3.6
H.3.3.7
H.3.3.8
H.3.3.9
H.3.4 Retort-kit cups
H.3.4.1
H.3.4.2
H.3.4.3
H.3.4.4
H.3.4.5
H.3.5 Filter press gasket and O-rings
H.3.5.1
H.3.5.2
H.3.5.3
Annex I
I.1 Principle
I.1.1
I.1.2
I.2 Safety considerations
I.2.1
I.2.2
I.2.3
I.2.4
I.2.5
I.2.5.1
I.2.5.2
I.2.5.3
I.2.6
I.2.6.1
I.2.6.2
I.2.6.3
I.2.6.4
I.2.7
I.2.7.1
I.2.7.2
I.2.8
I.2.8.1
I.2.8.2
I.2.9
I.2.9.1
I.2.9.2
I.2.9.3
I.2.9.4
I.3 Apparatus — Permeability-plugging apparatus (PPA) with set-screw-secured end caps
I.3.1
I.3.1.1
I.3.1.2
I.3.1.3
I.3.1.4
I.3.1.5
I.3.1.6
I.3.1.7
I.3.2
I.3.2.1
I.3.2.2
I.3.2.3
I.3.2.4
I.3.2.5
I.3.2.6
I.3.3
I.3.4
I.3.5
I.3.6
I.4 Procedure for high-temperature, high-pressure (HTHP) filtration
I.4.1 Preheating the heating jacket
I.4.1.1
I.4.1.2
I.4.1.3
I.4.2 Loading the filtration cell
I.4.2.1
I.4.2.2
I.4.2.3
I.4.2.4
I.4.2.5
I.4.2.6
I.4.2.7
I.4.2.8
I.4.2.9
I.4.2.10
I.4.2.11
I.4.2.12
I.4.2.13
I.4.3 Pressurizing the cell
I.4.3.1
I.4.3.2
I.4.3.3
I.4.3.4
I.4.3.5
I.4.3.6
I.4.3.7
I.4.4 Conducting the filtration test
I.4.4.1
I.4.4.2
I.4.4.3
I.4.4.4
I.4.4.5
I.5 Test conclusion and disassembly
I.5.1
I.5.2
I.5.3
I.5.4
I.5.5
I.5.6
I.5.7
I.5.7.1
I.5.7.2
I.5.8
I.5.9
I.5.10
I.5.11
I.5.12
I.5.13
I.6 Test reports
I.6.1 Filtrate reporting
I.6.2 Spurt loss
I.6.3 Calculation
I.6.4 Test report for filter cake
Annex J
J.1 Principle
J.1.1
J.1.2
J.2 Safety considerations
J.2.1
J.2.2
J.2.3
J.2.4
J.2.5
J.2.5.1
J.2.5.2
J.2.5.3
J.2.6
J.2.6.1
J.2.6.2
J.2.6.3
J.2.6.4
J.2.7
J.2.7.1
J.2.7.2
J.2.8
J.2.8.1
J.2.8.2
J.2.9
J.2.9.1
J.2.9.2
J.2.9.3
J.3 Apparatus — Permeability plugging apparatus (PPA) with threaded end caps
J.3.1
J.3.1.1
J.3.1.2
J.3.1.3
J.3.1.4
J.3.1.5
J.3.1.6
J.3.1.7
J.3.1.8
J.3.2
J.3.2.1
J.3.2.2
J.3.2.3
J.3.2.4
J.3.2.5
J.3.2.6
J.3.2.7
J.3.3
J.3.4
J.3.5
J.3.6
J.4 Procedure for high-temperature/high-pressure (HTHP) filtration
J.4.1 Preheating the heating jacket
J.4.1.1
J.4.1.2
J.4.1.3
J.4.2 Loading the filtration cell
J.4.2.1
J.4.2.2
J.4.2.3
J.4.2.4
J.4.2.5
J.4.2.6
J.4.2.7
J.4.2.8
J.4.2.9
J.4.2.10
J.4.2.11
J.4.2.12
J.4.2.13
J.4.2.14
J.4.2.15
J.4.3 Pressurizing the cell
J.4.3.1
J.4.3.2
J.4.3.3
J.4.3.4
J.4.3.5
J.4.3.6
J.4.3.7
J.4.4 Conducting the filtration test
J.4.4.1
J.4.4.2
J.4.4.3
J.4.4.4
J.4.4.5
J.4.4.6
J.5 Test conclusion and disassembly
J.5.1
J.5.2
J.5.3
J.5.4
J.5.5
J.5.6
J.5.7
J.5.8
J.5.9
J.5.10
J.5.11
J.5.12
J.5.13
J.5.14
J.5.15
J.5.16
J.6 Test reports
J.6.1 Filtrate reporting
J.6.2 Spurt loss
J.6.3 Calculation
J.6.4 Filter cake reporting
Annex K
Bibliography
Cited references in this standard
Please select a variation to view its description.
| Published | 09/09/2022 |
|---|---|
| Pages | 95 |
Please select a variation to view its pdf.
